The preparation of ester heterocycles mostly uses heteroatoms as nucleophilic sites, which are achieved by intramolecular substitution or addition reactions. Compound: 1-(4-(4-Hydroxyphenyl)piperazin-1-yl)ethanone( cas:67914-60-7 ) is researched.Safety of 1-(4-(4-Hydroxyphenyl)piperazin-1-yl)ethanone.Nematollahi, Davood; Amani, Amene published the article 《Electrochemical synthesis of the new substituted phenylpiperazines》 about this compound( cas:67914-60-7 ) in Journal of Electroanalytical Chemistry. Keywords: phenylpiperazine derivative electrooxidation electrosynthesis arylsulfinic acid. Let’s learn more about this compound (cas:67914-60-7).
Electrochem. oxidation of 1-(4-(4-hydroxyphenyl)piperazin-1-yl)ethanone (1) has been studied in the presence of arylsulfinic acids (3a-c) as nucleophiles in aqueous solutions using cyclic voltammetry and controlled-potential coulometry methods. The results revealed that quinone-imine derived from oxidation of 1 participates in Michael type addition reaction with arylsulfinic acids and via an EC mechanism converts to the corresponding new phenylpiperazine derivatives The present work has led to the development of a facile and environmentally friendly reagent-less electrochem. method for synthesis of some new phenylpiperazine derivatives in aqueous solutions with high atom economy and safe waste under ambient conditions and in an undivided cell using a carbon electrode.
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Reference:
Oxazolidine – Wikipedia,
Oxazolidine | C3H7NO – PubChem