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alpha-Amino Acid Derivatives as Chiral Educts for Asymmetric Products. Synthesis of Shpingosine from alpha’-Amino-alpha,beta-ynones

The utility of alpha’-amino-alpha,beta-ynones in the chirospecific synthesis of sphingosine is demonstrated.Thus, a protected L-serine isoxazolidide has been converted to sphingosine by two routes, both via alpha,beta-ynones.The first route is very short and high yielding, merely involving two selective reductions after synthesis the appropriate alpha,beta-ynone.The second route involves alkylation of a beta-unsubstituted ynone and illustrates the synthetic versatility of the alpha’-amino-alpha,beta-ynone system.Further routes through conjugate 1,4-additions to ynones are demonstrated but are limited by the highly reactive nature of this system.

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Reference£º
Oxazolidine – Wikipedia,
Oxazolidine | C3H1277NO – PubChem

 

Simple exploration of 583-47-1

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Related Products of 583-47-1, Because a catalyst decreases the height of the energy barrier, its presence increases the reaction rates of both the forward and the reverse reactions by the same amount.583-47-1, Name is 4-Benzyloxazolidine-2,5-dione, molecular formula is C10H9NO3. In a article£¬once mentioned of 583-47-1

A new simple and quantitative synthesis of alpha-aminoacid-N-carboxyanhydrides (oxazolidines-2,5-dione)

Nitrosation of chiral N-carbamoylaminoacids with a mixture of NO and O2 gives, with the same configuration and in quantitative yield the corresponding alpha-aminoacid-N-carboxyanhydrides (NCA), well known precursors of peptides. The by products of this reaction are N2 and H2O. Copyright (C) 1996 Elsevier Science Ltd.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H2203NO – PubChem

 

Brief introduction of 5,5-Dimethyloxazolidine-2,4-dione

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Electric Literature of 695-53-4, A catalyst don’t appear in the overall stoichiometry of the reaction it catalyzes, but it must appear in at least one of the elementary reactions in the mechanism for the catalyzed reaction. 695-53-4, Name is 5,5-Dimethyloxazolidine-2,4-dione, molecular formula is C5H7NO3. In a Article£¬once mentioned of 695-53-4

SYNTHESIS OF 13-AZA-16-OXA-, 13-AZA-16-THIA- AND 13,16-DIAZASTEROIDAL COMPOUNDS THROUGH CYCLIZATION OF N-ACYLIMINIUM ION INTERMEDIATES

5,5-Dimethyl-2,4-oxazolidinedione, 2,4-thiazolidinedione and 5,5-dimethylhydantoin were coupled with 2-(3,4-dihydro-1-naphthyl)ethyl alcohol by an application of Mitsunobu’s method to give the corresponding N-substituted products (5)-(7), respectively.Reduction of 5 – 7 with diisobutylaluminium hydride, followed by cyclization of the reduction products with formic acid yielded the 13-aza-16-oxa- (11), 13-aza-16-thia- (12) and 13,16-diaza-1,3,5(10),9(11)-estratetraen-17-one (13), respectively.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H1364NO – PubChem

 

Extracurricular laboratory:new discovery of 497-25-6

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Inverse Electron-Demand [4 + 2]-Cycloadditions of Ynamides: Access to Novel Pyridine Scaffolds

Functionalized polycyclic aminopyridines are central to the chemical sciences, but their syntheses are still hampered by a number of shortcomings. These nitrogenated heterocycles can be efficiently prepared by an intramolecular inverse electron demand hetero Diels-Alder (ihDA) cycloaddition of ynamides to pyrimidines. This ihDA/rDA sequence is general in scope and affords expedient access to novel types of aminopyridinyl scaffolds that hold great promise in terms of exit vector patterns.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H507NO – PubChem

 

Discovery of Oxazolidin-2-one

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A Robust One-Step Approach to Ynamides

A robust one-step synthetic strategy for ynamide with cheap and easily available stock chemicals vinyl dichlorides and electron deficient amides as the starting material is described. In the absence of transition-metal catalyst, the reaction proceeds under mild reaction conditions in open air and thus rendering a convenient operation. This strategy is not only suitable for both terminal and internal ynamide synthesis but also amenable for large-scale preparation. Broad substrate scopes with respect to vinyl dichloride as well as electron-deficient amide were observed.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H1075NO – PubChem

 

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Hypervalent organoantimony and -bismuth compounds with pendant arm ligands

Recent developments in chemistry of hypervalent organoantimony and -bismuth complexes with bidentate (C,E)- and tridentate (E,C,E)- and (C,E,C)-ligands are reviewed. The ligands are bonded to the antimony or bismuth atoms through carbon atoms and through intramolecular coordination with dative bonds from nitrogen, oxygen or sulfur atoms. Syntheses, structures including chirality aspects, reactions, fluxional behavior, biological aspects and applications in the field of catalysis and organic syntheses are considered in this review.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H922NO – PubChem

 

Archives for Chemistry Experiments of (R)-4-Benzyl-2-oxazolidinone

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Iodocyclization of ethoxyethyl ethers to ynamides: An immediate construction to benzo[ b ]furans

The iodocyclization of ethoxyethyl ethers to ynamides was completed within three seconds. The corresponding benzo[b]furans were obtained in high yields (84%-quant.) under mild conditions.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H1966NO – PubChem

 

Top Picks: new discover of Oxazolidin-2-one

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Method of treating cancer

The present invention relates to methods of treating cancer using a combination of a compound which is an antineoplastic agent and a compound which is a inhibitor of prenyl-protein transferase, which methods comprise administering to said mammal, either sequentially in any order or simultaneously, amounts of at least two therapeutic agents selected from a group consisting of a compound which is an antineoplastic agent and a compound which is a inhibitor of prenyl-protein transferase. The invention also relates to methods of preparing such compositions.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H179NO – PubChem

 

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Recent progress in the discovery and development of DNA gyrase B inhibitors

New antibacterials that modulate less explored targets are needed to fight the emerging bacterial resistance. DNA gyrase and topoisomerase IV are attractive targets in this search. These are both type II topoisomerases that can cleave both DNA strands, and can thus alter DNA topology during replication or similar processes. Currently, there are no ATP-competitive inhibitors of these two enzymes on the market, as the only aminocoumarin representative, novobiocin, was withdrawn due to safety concerns. The search for novel ATP-competitive inhibitors is a focus of ongoing industrial and academical research. This review summarizes the recent efforts in the design, synthesis and evaluation of GyrB/ParE inhibitors. The various approaches to achieve improved antibacterial activities are described, with particular reference to Gram-negative bacteria.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H335NO – PubChem

 

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Process for the manufacture of alkyl compounds

Process for the manufacture of a compound of formula I wherein R1 is H, acyl, alkyl or carbamoyl, R2 is a linear alkyl or alkenyl group, preferably a linear alkyl group comprising from 6 to 20 carbon atoms and n is 0, 1, 2, or 3, which comprises reacting a compound of formula II wherein R1 and n are as above and X is a leaving group with a carbanionic reagent of formula II ???????? M-R2 wherein R2 is as above and M denotes a metal or a metal containing group.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H205NO – PubChem