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PROCESS FOR THE PREPARATION OF ZOLMITRIPTAN, SALTS AND SOLVATES THEREOF

The present invention relates to an improved process for the preparation of the active pharmaceutical ingredient zolmitriptan. In particular, it relates to an efficient process for the preparation of zolmitriptan and its pharmaceutically acceptable salts and solvates.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H2211NO – PubChem

 

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Pyrrolizidine alkaloids: Occurrence, biology, and chemical synthesis

Covering: 2013 up to the end of 2015 This review covers the isolation and structure of new pyrrolizidines; pyrrolizidine biosynthesis; biological activity, including the occurrence of pyrrolizidines as toxic components or contaminants in foods and beverages; and formal and total syntheses of naturally-occurring pyrrolizidine alkaloids and closely related non-natural analogues.

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Oxazolidine – Wikipedia,
Oxazolidine | C3H1244NO – PubChem

 

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Heterogeneously catalyzed selective aerobic oxidative cross-coupling of terminal alkynes and amides with simple copper(ii) hydroxide

Simple copper(ii) hydroxide Cu(OH)2 could act as an efficient heterogeneous catalyst for selective oxidative cross-coupling of a broad range of terminal alkynes and amides using air as a sole oxidant, giving the corresponding ynamides in moderate to high yields (56-93% yields). The Royal Society of Chemistry 2012.

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Oxazolidine – Wikipedia,
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Formation of enamides via palladium(II)-catalyzed vinyl transfer from vinyl ethers to nitrogen nucleophiles

Matrix presented. Palladium(II) complexes catalyze the formation of enamides via the formal cross-coupling reaction between nitrogen nucleophiles and vinyl ethers. These vinyl transfer reactions proceed in good yields with amide, carbamate, and sulfonamide nucleophiles, and the optimal catalyst is (DPP)Pd(OCOCF3)2 (DPP = 4,7-diphenyl-1,10-phenanthroline).

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Oxazolidine – Wikipedia,
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Phase-transfer catalyzed asymmetric arylacetate alkylation

Phenethyl arylacetates are alkylated under phase-transfer conditions with cinchona catalysts with alkyl halides in high yield with excellent enantioselectivity (84-99% ee) following recrystallization. Cinchonidine (CD) derived catalyst gave the (R)-product and cinchonine (CN) catalyst produced the (S)-product. The phenethyl (PE) ester group is removed, using ammonium formate and catalytic Pd/C, to give alkylated carboxylic acid products in high selectivity. The utility of the approach is demonstrated by a direct synthesis of (S)-naproxen.

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Chemistry is traditionally divided into organic and inorganic chemistry. Application In Synthesis of (S)-N-Boc-2,2-dimethyloxazolidine-4-carboxylic Acid, The former is the study of compounds containing at least one carbon-hydrogen bonds.In a patent£¬Which mentioned a new discovery about 139009-66-8

COMBRETASTATIN DERIVATIVE PREPARATION METHOD

The invention relates to a method for preparing a combretastatin derivative (I) or (II), said method including the following steps: triaryl(3,4,5-trimethoxybenzyl)phosphonium halide P3 (III), wherein Ar denotes an aryl group selected from among phenyl or thienyl, is reacted with P2 having formula (IV) or P?2 having formula (V) so as to respectively obtain the compound P4 or P?4, which have formulas (VI) and (VII), respectively; then, during a step for deprotection in the presence of an acid and/or a base, the compound having P4 or P?4 leads, after an optional purification step, to the compound having formula (I) or (II).

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Oxazolidine – Wikipedia,
Oxazolidine | C3H2355NO – PubChem

 

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The chemistry and biology of rhizoxins, novel antitumor macrolides from Rhizopus chinensis

This Report reviews completed syntheses of the potent cytotoxic fungal metabolite rhizoxin and its natural congener didesepoxyrhizoxin (rhizoxin D) along with current knowledge of the pharmacological properties of these compounds.

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Promotion of reaction of N-H bonds with triarylbismuth and cupric acetate

Arylation of a diverse group of N-H containing compounds at room temperature with triarylbismuth and cupric acetate in the presence of a tertiary amine promoter, such as triethylamine or pyridine, is described. This mild and highly efficient procedure, which is based on Barton’s earlier work on the arylation of amines, can be applied to amides, imides, ureas, carbamates, and sulfonamides. Copyright (C) 1996 Elsevier Science Ltd.

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3-ISOXAZOLIDONE FROM JACK BEAN SEEDLINGS

Key Word Index – Canavalia ensiformis; Leguminosae; jack bean; 3-isoxazolidone; L-canavanine; L-canaline; pentacyanoammoniferrate reagent; Jaffe reagent. 3-Isoxazolidone has been isolated from jack bean seedlings.

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Unified approach to the asymmetric synthesis of higher homologues of (3-quinolyl)-alanine

A new protocol based on a palladium-catalyzed Heck reaction of an amino acid-derived vinyl unit with 3-bromoquinoline has been developed to access the title compounds in good yield and optical purity. Copyright

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Oxazolidine – Wikipedia,
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